PHOSPHORUS OXYCHLORIDE – SAFETY DATA SHEET PAGE 11

Safety Data Sheet (Effective Date: October 30, 2013)

PHOSPHORUS OXYCHLORIDE

SECTION 1. IDENTIFICATION

SECTION 2. HAZARD(S) IDENTIFICATION

HAZCOM Standard Status: This material is considered hazardous by the OSHA Hazard Communication Standard (29CFR 1910.1200)

Physical state: Liquid.

Color: Colorless.

Classification of the ACUTE TOXICITY: ORAL - Category 4

Substance or mixture: ACUTE TOXICITY: INHALATION - Category 2

SKIN CORROSION/IRRITATION - Category 1

SERIOUS EYE DAMAGE/ EYE IRRITATION - Category 1

SPECIFIC TARGET ORGAN TOXICITY (SINGLE EXPOSURE): INHALATION [lungs]–Category 1

Hazard pictograms:

Signal word: Danger

Hazard statements: Fatal if inhaled. Harmful if swallowed. Causes sever skin burns and eye damage. Causes damage to organs

Hazard Not Otherwise Water Reactive. Reacts with water to release toxic gas, which may be fatal Classified (HNOC): inhaled. Causes digestive tract burns.

Precautionary Statements

Prevention: Wear respiratory protection. Wear protective gloves/clothing and eye/face protection.

Use only in a well-ventilated area. Do not breathe vapor. Do not eat, drink or smoke when using this product. Wash hands thoroughly after handling.

Response: IF INHALED: Remove victim to fresh air and keep at rest in a position comfortable for breathing. IF SWALLOWED: Rinse mouth. Do NOT induce vomiting. IF ON SKIN (or hair): Take off immediately all contaminated clothing. Rinse skin with water or shower. Wash contaminated clothing before reuse. IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing. Get medical attention immediately.

Storage: Store locked up.

Disposal: Dispose of contents and container in accordance with all local, regional, national and international regulations.

SECTION 3. COMPOSITION/INFORMATION ON INGRIDIENTS

Substance/mixture: Substance

Chemical name: PHOSPHORUS OXYCHLORIDE

Synonyms: Phosphoryl chloride, Phosphorus oxytrichloride

Chemical Formula: POCl3

CAS# 10025-87-3

UN# 1810

ICSC# 0190

C.C.C. Mark 28121090307

CC List 1C350c.3

There are no additional ingredients present which, within the current knowledge of the supplier and in the concentrations applicable, are classified as hazardous to health and hence require reporting in this section.

SECTION 4. FIRST AID MEASURES

Description of first aid measures

Potential acute health effects

section 5. fire-fighting measures

Extinguishing media

section 6. accidental release measures

section 7. handling and storage

Precautions for safe handling

section 7. handling and storage (con’t)

section 8. exposure controls/personal protection

Occupational exposure limits

INGRIDIENT NAME / EXPOSURE LIMITS
Phosphorus oxychloride / ACGIH TLV (United States, 3/2012
TWA: 0.1 ppm 8 hourTWA .63 mg/m3 8 hours

If this product contains ingredients with exposure limits, personal, workplace atmosphere or biological monitoring may be

required to determine the effectiveness of the ventilation or other control measures and/or the necessity to use respiratory protective equipment.

Personal protection

section 8. exposure controls/personal protection (con’t)

section 9. physical and chemical properties

section 10. stability and reactivity

section 10. stability and reactivity (con’t)

section 11. toxicological information

Potential acute health effects

Symptoms related to the physical, chemical and toxicological characteristics

Potential chronic health effects

Short term exposure

Long term exposure

Information on toxicological effects

Acute toxicity

Product/ingredient name / Result / Species / Dose / Exposure / Test
Phosphorus Oxychloride / LD50 Oral / Rat / 304 to 475 mg/kg / _ / _
Phosphorus Oxychloride / LC 50 inhalation
Dusts and mists / Rat / .303 mg/l / 4 hours / _

section 11. toxicological information (con’t)

Irritation/Corrosion

Conclusion/Summary

Chronic toxicity

Product/ingredient name / Result / Species / Dose / Exposure
Phosphorus oxychloride / Sub-chronic NOAEL Oral / Rat / 19.3mg/kg daily / _

Mutagenicity

Product/ingredient name / Test / Experiment / Result
Phosphorus Oxychloride / OECD 471 Bacterial Reverse Mutation Test: with metabolic activation/without metabolic activation / Experiment: in vitro
Subject: Bacteria / Negative

Carcinogenicity

Product/ingredient name / CAS # / IARC / NTP / OSHA
Phosphorus Oxychloride / 10025-87-3 / Not classified / Not classified / Not classified
Product/ingredient name / Maternal Toxicity / Species / Dose / Exposure
Phosphorus Oxychloride / Rat / Oral: 19.3 mg/kg / _

Specific target organ toxicity (single exposure)

Product/ingredient name / Category / Route of exposure / Target organs
Phosphorus oxychloride / Category 1 / Inhalation / lungs

section 12. ecological information

Toxicity

Product/ingredient name / Test / Result / Species / Exposure
Phosphorus Oxhchloride / OECD 202 Daphnia sp. Acute Immobilization test
OECD 201
Freshwater Alga and Cyanobacteria, Growth Inhibition Test (biomass)
OECD 201
Freshwater Alga and cyanobacteria, Growth Inhibition Test (growth rate)
OICD 203 Fish, Acute Toxicity Test / Acute EC50 35.04 mg/l Fresh water
Acute IC50 27.91 mg/l (biomass) Fresh water
Acute IC50 32.12 mg/l (growth rate) Fresh water
Acute LC 50> 1000 mg/l Fresh water / Daphnia – Daphnia magma
Algae – Desmodesmus subspicatus
Algae- Desmodesmus subspicatus
Fish – Danio rerio / 48 hours
72 hours
72 hours
96 hours
Product/ingredient name / Test (con’t) / Result (con’t) / Species (con’t) / Exposure (con’t)
Phosphorus Oxychloride / OECD 201
Freshwater Alga and Cyanobacteria, Growth Inhibition Test / Acute NOEC 12.5 mg/l Fresh water / Algae – Desmodesmus subspicatus / 72 hours

Conclusion/Summary Not available.

Persistence and degradability

Conclusion/Summary Not available.

Bioaccumulative potential

Not Available

Mobility in Soil

Soil/water partition Not available

coefficient (KOC)

Other adverse effects No known significant effects or critical hazards

SECTION 13. DISPOSAL CONSIDERATIONS

SECTION 14. TRANSPORT INFORMATION

Regulatory information / UN # / Proper shipping name / Classes / PG* / Label / Additional information
DOT Classification / UN1810 / Phosphorus Oxychloride / 6.1 (8) / 1 / / Poison Inhalation Hazard – Hazard Zone B
IMDG Class / UN1810 / Phosphorus Oxychloride / 6.1 (8) / 1 / / Emergency schedules (EmS)
F-A, S-B
IATA-DGR Class / Forbidden

PG* Packing Group

RQ: 993 lbs

SECTION 15. REGULATORY INFORMATION

State Regulations

The following chemicals are specifically listed by individual states; other product specific health and safety data in other

sections on the SDS may also be applicable for state requirements. For details on your regulatory requirements you

should contact the appropraite agency in your state.

Ingredient name CAS number State Code Concentration

Phosphorus oxychloride 10025-87-3 MA - S, NJ - HS, PA - RTK HS >99.7

Massachusetts Substances: MA - S

Massachusetts Extraordinary Hazardous Substances: MA - Extra HS

New Jersey Hazardous Substances: NJ - HS

Pennsylvania RTK Hazardous Substances: PA - RTK HS

Pennsylvania Special Hazardous Substances: PA - Special HS

California Prop. 65

To the best of our knowledge, this product does not contain any of the listed chemicals, which the state of California has

found to cause cancer, birth defects or other reproductive harm.

U.S. Toxic Substances Listed on TSCA Inventory

Control Act

Section 16. OTHER INFORMATION

The customer is responsible for determining the PPE code for this material. HMIS® ratings are to be used with a fully implemented HMIS® program. HMIS® is a registered mark of the National Paint & Coatings Association (NPCA).

xSi’s method of hazard communication is comprised of Product Labels and Safety Data Sheets. HMIS and NFPA ratings are provided as a customer service.

Notice to reader

This information is furnished without warranty, express or implied. This information is based on information provided by the manufacturer to xSi and is believed by xSi to be accurate. The information in this SDS relates only to the specific material designated herein. xSi assumes no legal responsibility for use of or reliance upon the information in this SDS.