H.E.J. RESEARCH INSTITUTE OF CHEMISTRY

INTERNATIONAL CENTER FOR CHEMICAL SCIENCES

UNIVERSITY OF KARACHI, KARACHI-75270

Sponsored by the Higher Education Commission and Private Institutions Analyses

Sample Submission Form

Date:

Name:

Name of Organization:

Address:

Sample code: …………………………………………. Type of analysis:……………………….……………

(Please use separate form for each sample for each technique)

M.P./B.P.: ……….. Solvent for analysis

TLC purity: TLC solvent system:

Molecular weight/Molecular formula (if known):

Solvent for NMR analysis: CDCl3/DMSO/D2O/

Solubility at 25o C:

Nature of sample (i.e. steroid, alkaloid etc):

Any other information:………………………………………………………………………………...

Ø  For NMR analysis, at least 20 mg of substance is required with complete solubility in approximately 0.5 mL of some common deuterated solvent.

Ø  Quantity, solubility and purity of the substance submitted should be checked carefully. Kindly make sure that it is organic in nature and not a quaternary salt, betaine or a metal complex.

Ø  The bill will be sent to the HEC under the “Access to Scientific Instrument Program.”

Signature and Seal of Chairperson/Director of Institution……… ……………………………………………

Approval of the Director HEJRIC: …………………………………………………………………..

Received: Date: No.:

Completed: Date: Signature:

Signature of Section Incharge:

INTERNATIONAL CENTER FOR CHEMICAL AND BIOLOGICAL SCIENCES (HEJ RESEARCH INSTITUTE OF CHEMISTRY, DR. PANJWANI CENTER FOR MOLECULAR MEDICINE AND DRUG RESEARCH) UNIVERSITY OF KARACHI-75270, PAKISTAN. Page 1of 2
S. No. / TYPE OF ANALYSIS / DISCOUNTED RATES FOR PUBLIC SECTOR INSTITUTIONS
Pak Rupees.
1 / a. / PROTON NMR SPECTRA (D2O OR CDCl3) / 2,500.00
b. / IN ANY OTHER DEUTERATED SOLVENT / 5,000.00
2 / CARBON 13 NMR SPECTRA
BROAD BAND DECOUPLED SPECTRUM
a. / IN D2O OR CDCl3 / 5,000.00
b. / IN ANY OTHER DEUTERATED SOLVENT / 7,000.00
3 / OFF-RESONANCE SPECTRUM
a. / IN CDCl3 / 6,000.00
b. / IN ANY OTHER DEUTERATED SOLVENT / 8,000.00
4 / INVERSE NMR MEASUREMENTS HMBC,HMQC, HSQC, etc.
a. / IN D2O OR CDCl3 / 6,000.00
b. / IN ANY OTHER DEUTERATED SOLVENT / 12,000.00
5 / HOMONUCLEAR 2 D- COSY,NOESY,TOCSY,DOSY,ROESY
a. / IN D2O OR CDCl3 / 2,500.00
b. / IN ANY OTHER DEUTERATED SOLVENT / 5,000.00
6 / 2D INADEQUATE
a. / IN D2O OR CDCl3 / 5,000.00
b. / IN ANY OTHER DEUTERATED SOLVENT / 10,000.00
7 / J-RES, X-J-RES
a. / IN D2O OR CDCl3 / 5,000.00
b. / IN ANY OTHER DEUTERATED SOLVENT / 7,000.00
8 / NOE DIFFERENCE
a. / IN D2O OR CDCl3 (PER EXPERIMENT) / 2,500.00
b. / IN ANY OTHER DEUTERATED SOLVENT (PER EXPERIMENT) / 5,000.00
9 / 1-D SELECTIVE COSY, NOESY ,TOCSY
a. / IN D2O OR CDCl3 (PER EXPERIMENT) / 2,500.00
b. / IN ANY OTHER DEUTERATED SOLVENT (PER EXPERIMENT) / 5,000.00
IF SAMPLE IS NOT SOLUBLE IN SPECIFIED
SOLVENT(FOR EACH DEUTERATED SOLVENT) / 3,000.00
10 / SINGLE -CRYSTAL X-RAY DIFFRACTION ANALYSIS / 10,000.00
11 / UV SPECTRUM / 500.00
12 / IR SPECTRUM / 1,000.00
13 / GAS CHROMOTOGRAPHIC ANALYSIS / 5,000.00
14 / CD SPECTRUM / 1,000.00
15 / C.H.N. MICROANALYSIS / 6,000.00
Page 2 of 2
S. No. / TYPE OF ANALYSIS / DISCOUNTED RATES FOR PUBLIC SECTOR INSTITUTIONS
16 / OPTICAL ROATATION / Rs. 200.00
17 / EI, POSITIVE MODE / 5,000.00
18 / HR-EI POSITIVE MODE / 8,000.00
19 / CI POSITIVE NEGATIVE MODE / 7,000.00
20 / GCMS-EI, POSITIVE MODE, FULL SCAN / 15,000.00
21 / FAB POSITIVE/NEGATIVE MODE / 6,000.00
22 / FAB-HR (PEAK MATCHING) POSITIVE/NEGATIVE / 7,000.00
23 / ESI-HR-MS,POSITIVE/NEGATIVE / 8,000.00
24 / ESI-HR-MSMS,POSITIVE/NEGATIVE / 12,000.00
25 / LCMS-ESI, POSITIVE/NEGATIVE, FULL SCAN / 18,000.00
26 / MALDI,POSITIVE/NEGATIVE / 12,000.00
IMAGING FACILITY
27 / DIC AND BRIGHT FIELD MICROSCOPY AND
IMAGE CAPTURING / 1,000.00
28 / FLORESCENT MICROSCOPY AND
IMAGE CAPTURING / 2,000.00
29 / DIC AND BRIGHT FIELD MICROSCOPY AND
IMAGE CAPTURING / 1,000.00
FLORESCENT MICROSCOPY AND
30 / IMAGE CAPTURING / 2,000.00
TISSUE PROCESSING,EMBEDDING,SECTIONING AND
31 / H&E STAINING ANIMAL / 1,000.00
32 / ATOMIC FORCE MICROSCOPY (AFM) / 3,000.00
Note: Samples must be submitted ready for direct analysis as single pure ingredients with their solubility in CDCl3 for NMR and MeOH for UV. If the material is not soluble in chloroform then the solubility in other solvents must be pre-checked and the solvent in which the spectrum is to be recorded clearly specified. The above rates are applicable for government institution only. Private institutions would be charged 100% extra. For peak matching and High Resolution Measurements; low resolution (EI or FAB) spectra are required.